Synthesis, structural and magnetic characterization of soft magnetic nanocrystalline ternary FeNiCo particles
Artikel i vetenskaplig tidskrift, 2017

The present study focuses on the synthesis, microstructural and magnetic properties of ternary FeNiCo nanoparticles. Nanocrystalline ternary FeNiCo particles were synthesized via hydrogen reduction assisted ultrasonic spray pyrolysis method in single step. The effect of precursor concentration on the morphology and the size of particles was investigated. The syntheses were performed at 800 °C. Structure, morphology and magnetic properties of the as-prepared products were characterized through X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and vibrating sample magnetometer (VSM) studies. Scherer calculation revealed that crystallite size of the ternary particles ranged between 36 and 60 nm. SEM and TEM investigations showed that the particle size was strongly influenced by the precursor concentration and Fe, Ni, Co elemental composition of individual particles was homogeneous. Finally, the soft magnetic properties of the particles were observed to be a function of their size.

Ultrasonic spray pyrolysis

Electron microscopy

Hydrogen reduction

Magnetic properties

FeNiCo nanoparticles

Magnetic materials

Författare

Cigdem Toparli

Max Planck-institutet

Istanbul Teknik Universitesi

Burcak Ebin

Industriell materialåtervinning

S. Gurmen

Istanbul Teknik Universitesi

Journal of Magnetism and Magnetic Materials

0304-8853 (ISSN)

Vol. 423 133-139

Ämneskategorier

Materialkemi

DOI

10.1016/j.jmmm.2016.09.005